Abstract
| Lingua originale | English |
|---|---|
| Numero di pagine | 5 |
| Rivista | Natural Product Research |
| Stato di pubblicazione | Published - 2016 |
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All Science Journal Classification (ASJC) codes
- Analytical Chemistry
- Biochemistry
- Plant Science
- Organic Chemistry
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Analysis of β2-agonists in cattle hair samples using a rapid UHPLC–ESI–MS/MS method. / Di Stefano, Vita; Ferrantelli, Vincenzo; Cicero, Nicola; Macaluso, Andrea; Alongi, Angelina; Giaccone, Vita; Pitonzo, Rosa.
In: Natural Product Research, 2016.Risultato della ricerca: Article
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TY - JOUR
T1 - Analysis of β2-agonists in cattle hair samples using a rapid UHPLC–ESI–MS/MS method
AU - Di Stefano, Vita
AU - Ferrantelli, Vincenzo
AU - Cicero, Nicola
AU - Macaluso, Andrea
AU - Alongi, Angelina
AU - Giaccone, Vita
AU - Pitonzo, Rosa
PY - 2016
Y1 - 2016
N2 - A simple and efficient method was developed for simultaneousanalysis of five illegal residual β2-agonists in cattle hair. β2-Agonistswere quantified by ultra high performance liquid chromatographycoupled with electrospray ionisation tandem mass spectrometryoperating in positive multiple-reaction monitoring mode. The methodwas validated as quantitative confirmatory method according to theEU Decision 2002/657/EC: instrumental linearity, specificity, precision,recovery, decision limit (CCα) and detection capability (CCβ) wereevaluated. The recovery were greater than 90% and the methodappeared suitable for the control of these β2-agonists in cattle hairsamples with LOQ values between 4.9 and 5.5 μg/kg. This methodcould represent a simple and cheap approach to confirm β2-agonistscontamination of cattle for feeding in a not invasive way and beforeslaughter operations.
AB - A simple and efficient method was developed for simultaneousanalysis of five illegal residual β2-agonists in cattle hair. β2-Agonistswere quantified by ultra high performance liquid chromatographycoupled with electrospray ionisation tandem mass spectrometryoperating in positive multiple-reaction monitoring mode. The methodwas validated as quantitative confirmatory method according to theEU Decision 2002/657/EC: instrumental linearity, specificity, precision,recovery, decision limit (CCα) and detection capability (CCβ) wereevaluated. The recovery were greater than 90% and the methodappeared suitable for the control of these β2-agonists in cattle hairsamples with LOQ values between 4.9 and 5.5 μg/kg. This methodcould represent a simple and cheap approach to confirm β2-agonistscontamination of cattle for feeding in a not invasive way and beforeslaughter operations.
UR - http://hdl.handle.net/10447/213269
M3 - Article
JO - Natural Product Research
JF - Natural Product Research
SN - 1478-6419
ER -